New Elaborated Technique for Isolation and Purification of Limonene from Orange Oil Isolation of limonene from orange oil
Iranian Journal of Pharmaceutical Sciences,
مجلد 2 عدد 2 (2006),
1 April 2006
,
الصفحة 87-90
https://doi.org/10.22037/ijps.v2.39555
الملخص
Essential oil of the orange peel which was extracted by hydrodistillation method showed 50 different mono- and sesquiterpenes on GC-MS analysis, in which
limonene had the highest percentage (92.4%). Due to various important uses of the compound, a method was developed for isolation and purification of limonene. In this method, for extra purification, a fractional distillation on Vigreux column under 100 mm Hg vacuum was used which resulted in 96.7% purity for limonene.
Subsequent chromatography by two different packages of silica gel and active charcoal columns resulted in 99.4% and 99.9 % purity of limonene, respectively.
- Column chromatography
- Fractional distillation
- Limonene
- Orange oil
- Vigreux
كيفية الاقتباس
المراجع
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- الملخص المشاهدات: 102 الأوقات
- IJPS_Volume 2_Issue 2_Pages 87-90 (English) التنزيلات: 21 الأوقات